Producing diamond anvil cell gaskets for ultrahigh-pressure applicationsusing an inexpensive electric discharge machine

نویسندگان

  • H. E. Lorenzana
  • M. B. Kruger
چکیده

Small holes are drilled in diamond anvil cell gaskets to contain and pressurize samples. As high-pressure technology pushes the multimegabar regime, smaller-tipped diamond anvils are being increasingly utilized. Consequently, well-centered holes with diameters smaller than 100 pm need to be routinely produced in these gaskets made of exceedingly hard metals. We describe the construction of an inexpensive electric discharge machine that can drill metals with holes as small as 25 pm in diameter. This method of drilling is easy to use, far less expensive than other commonly used techniques, and has the advantage of being effective on extremely difficult to machine metals such as rhenium.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

X-ray Imaging of Stress and Strain of Diamond, Iron, and Tungsten at Megabar Pressures

Synchrotron x-ray imaging and stress measurements of diamond-anvil cell gaskets revealed large elastic strains at the diamond tip at a pressure of 300 gigapascals. The diamond, generally considered a rigid body, bent 16 degrees over a distance of 300 micrometers without failure. To complement these measurements, a technique was developed that permits x-ray diffraction to be measured through a b...

متن کامل

Terapascal static pressure generation with ultrahigh yield strength nanodiamond

Studies of materials' properties at high and ultrahigh pressures lead to discoveries of unique physical and chemical phenomena and a deeper understanding of matter. In high-pressure research, an achievable static pressure limit is imposed by the strength of available strong materials and design of high-pressure devices. Using a high-pressure and high-temperature technique, we synthesized optica...

متن کامل

Density measurements of noncrystalline materials at high pressure with diamond anvil cell.

We describe an x-ray absorption method for in situ density measurement of non-crystalline materials in the diamond anvil cell using a monochromatic synchrotron x-ray microbeam. Sample thickness, which is indispensable in the absorption method, can be determined precisely by extrapolating the thickness profile of the gasket obtained by x-ray absorption and diffraction measurements. Diamond defor...

متن کامل

Laser heated diamond cell system at the Advanced Photon Source for in situ x-ray measurements at high pressure and temperature

We describe a laser heated diamond anvil cell system at the GeoSoilEnviroCARS sector at the Advanced Photon Source. The system can be used for in situ x-ray measurements at simultaneously ultrahigh pressures ~to .150 GPa! and ultrahigh temperatures ~to .4000 K!. Design goals of the laser heating system include generation of a large heating volume compared to the x-ray beam size, minimization of...

متن کامل

Suppression of Bragg reflection glitches of a single-crystal diamond anvil cell by a polycapillary half-lens in high-pressure XAFS spectroscopy.

In combination with a single-crystal diamond anvil cell (DAC), a polycapillary half-lens (PHL) re-focusing optics has been used to perform high-pressure extended X-ray absorption fine-structure measurements. It is found that a large divergent X-ray beam induced by the PHL leads the Bragg glitches from single-crystal diamond to be broadened significantly and the intensity of the glitches to be r...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:

دوره   شماره 

صفحات  -

تاریخ انتشار 1999